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林产化学与工业 ›› 2017, Vol. 37 ›› Issue (1): 141-148.doi: 10.3969/j.issn.0253-2417.2017.01.019

• 研究报告 • 上一篇    下一篇

不同产地香茅挥发油的化学成分比较研究

欧阳婷1, 杨琼梁1, 颜红1, 钟理峰1, 杨仁义2   

  1. 1. 湖南中医药大学 药学院, 湖南 长沙 410208;
    2. 湖南中医药大学 中西医结合学院, 湖南 长沙 410208
  • 收稿日期:2016-04-28 出版日期:2017-02-25 发布日期:2017-02-25
  • 通讯作者: 颜红,副教授,博士,硕士生导师,主要从事活性物质及药物新剂型的研究;E-mail:yh8632@126.com。 E-mail:yh8632@126.com
  • 作者简介:欧阳婷(1990-),女,湖南邵阳人,硕士生,从事天然产物研究及药物新剂型的开发工作
  • 基金资助:
    林业公益性行业科研专项(201404608);湖南省“中药学”重点学科项目(湘教通[2011]76号);湖南省研究生科研创新项目(CX2014B367)

Chemical Components Analysis of the Volatile Oil of Cymbopogon citrates (DC.) Stapf from Different Regions

OUYANG Ting1, YANG Qiongliang1, YAN Hong1, ZHONG Lifeng1, YANG Renyi2   

  1. 1. School of Pharmacy, Hunan University of Chinese Medicine, Changsha 410208, China;
    2. College of Integrated Traditional Chinese and Western Medicine, Hunan University of Chinese Medicine, Changsha 410208, China
  • Received:2016-04-28 Online:2017-02-25 Published:2017-02-25

摘要: 采用水蒸气蒸馏法提取香茅挥发油,利用气相色谱-质谱联用技术分别对5个不同产地香茅挥发油的化学组成进行了分析,并比较了不同部位之间挥发油化学成分的差异。结果表明:5个产地香茅均以叶的挥发油含量最高,其次为全草,茎的挥发油含量最低。不同产地香茅挥发油成分种类及其GC含量差异较大,湖南、广东、浙江、海南、福建香茅全草挥发油中分别鉴定出36、30、37、22和33种成分,叶挥发油分别鉴定出25、24、32、27和39种成分,主要成分均为(E)-柠檬醛、(Z)-柠檬醛、β-月桂烯、香叶醇等。5个产地香茅全草和叶挥发油中柠檬醛GC含量均最高,为70%~85%左右,其中(E)-柠檬醛为40.86%~51.15%,(Z)-柠檬醛为31.01%~36.46%;β-月桂烯GC含量为1.94%~15.43%,香叶醇GC含量为1.61%~4.89%。5个产地全草、叶挥发油中的成分主要为含氧单萜类(GC含量为81.91%~93.04%),含量具有地域性。

关键词: 香茅, 挥发油, 产地, 化学成分, 气相色谱-质谱

Abstract: The GC-MS technique was applied to analyze the volatile oil extracted by steam distillation from Cymbopogon citrates(DC.) Stapf that came from five different regions, and the chemical components of the volatile oil in different samples were compared. The results showed that in all five samples tested, the content of volatile oil in leaves was the highest, followed by the whole plant and then the stem. The types and contents of volatile components in C. citrates from different regions were different. The volatile oils in the whole plant from Hunan, Guangdong, Zhejiang, Hainan and Fujian were identified as 36, 30, 37, 22, 33 species components, respectively, and the volatile oils in the leaves were identified as 25, 24, 32, 27, 39 species components, respectively. The main constituents were identified as E-citral, Z-citral, β-myrcene and geraniol, etc. The volatile oil and whole plant has the highest amount of citral (about 70%-85%), with E-citral of 40.86%-51.15% and Z-citral of 31.01%-36.46%. The contents of β-myrcene and geraniol were 1.94%-15.43% and 1.61%-4.89%, respectively. The components of volatile oil in whole plant and leaves were mainly oxygenated monoterpenes (81.91%-93.04%) and with the characteristics of localization.

Key words: Cymbopogon citrates (DC.) Stapf, volatile oil, regions, chemical components, GC-MS

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