喷雾干燥法制备皱皮木瓜籽油微胶囊及其性能研究

doi:10.3969/j.issn.0253-2417.2018.01.005

林产化学与工业 ›› 2018, Vol. 38 ›› Issue (1): 33-38.doi: 10.3969/j.issn.0253-2417.2018.01.005

喷雾干燥法制备皱皮木瓜籽油微胶囊及其性能研究

邓叶俊¹, 黄立新^1,2, 张彩虹^1,2, 谢普军^1,2, 丁莎莎¹, 王晓杰¹

1. 中国林业科学研究院林产化学工业研究所;生物质化学利用国家工程实验室;国家林业局林产化学工程重点开放性实验室;江苏省生物质能源与材料重点实验室, 江苏南京 210042;
2. 中国林业科学研究院林业新技术研究所, 北京 100091

收稿日期:2017-06-13 出版日期:2018-02-25 发布日期:2018-02-28
通讯作者: 黄立新,研究员,博士生导师,研究领域为天然产物提取分离纯化及新型干燥技术;E-mail:l_x_huang@163.com。 E-mail:l_x_huang@163.com
作者简介:邓叶俊(1993-),男,安徽宣城人,硕士生,主要从事农林产品深加工;E-mail:yejun_deng@163.com
基金资助:
“十三五”国家重点研发计划资助（2017YFD0400902-3）；江苏省生物质能源与材料重点实验室资助（JSBEM-S-201507）

Preparation of Chaenomeles speciosa Seed Oil Microcapsule by Spray Drying Technology and Its Properties

DENG Yejun¹, HUANG Lixin^1,2, ZHANG Caihong^1,2, XIE Pujun^1,2, DING Shasha¹, WANG Xiaojie¹

1. Institute of Chemical Industry of Forest Products, CAF;National Engineering Lab. for Biomass Chemical Utilization;Key and Open Lab. of Forest Chemical Engineering, SFA;Key Lab. of Biomass Energy and Material, Jiangsu Province, Nanjing 210042, China;
2. Research Institute of Forestry New Technology, CAF, Beijing 100091, China

Received:2017-06-13 Online:2018-02-25 Published:2018-02-28

摘要/Abstract

摘要： 在单因素试验的基础上，利用正交试验探讨了皱皮木瓜籽油微胶囊制备的较佳工艺，结果表明：均质压力30 MPa，进风温度190℃，进料速率16 mL/min的条件下制备得到的微胶囊产品为淡黄色粉末，包埋率达83.59%，水分2.51%，密度0.625 g/cm³，吸水性9.191%，粒径39.440 μm。对微胶囊产品的SEM电镜结果显示：微胶囊产品呈球形，表面完整光滑，微胶囊结构致密。在贮藏稳定性试验中，皱皮木瓜籽油微胶囊的稳定性优于未包埋的皱皮木瓜籽油，喷雾干燥法制备的微胶囊产品性能优异，大大延长了皱皮木瓜籽油的货架期。

关键词: 皱皮木瓜籽油, 微胶囊, 喷雾干燥法, 稳定性

Abstract: Based on the single-factor experiments,orthogonal experiment was used to optimize the technical parameters for preparing Chaenomeles speciosa(Sweet) Nakai seed oil microcapsules and the optimum technical paramenters were as follows:homogeneous pressure 30 MPa,inlet temperature 190℃,feeding rate 16 mL/min.The microcapsules produced under these processing parameters were determined as canary yellow powders,with microencapsulation efficiency 83.59%,water content 2.51%,density 0.625 g/cm³,hygroscopicity 9.191%,and particle size 39.440 μm.The microcapsule powders observed by SEM were found to have regular spherical shape with smooth surface and compact structure.The results of storage stability study showed that the microcapsules were more stable against oxidation in air than the oil which was not entrapped.The properties of microcapsule products were excellent,and the shelf life of C.Speciosa seed oil was greatly extended.

Key words: Chaenomeles speciosa seed oil, microcapsule, spray drying technology, stability

中图分类号:

TQ35
TS224

邓叶俊, 黄立新, 张彩虹, 谢普军, 丁莎莎, 王晓杰. 喷雾干燥法制备皱皮木瓜籽油微胶囊及其性能研究[J]. 林产化学与工业, 2018, 38(1): 33-38.

DENG Yejun, HUANG Lixin, ZHANG Caihong, XIE Pujun, DING Shasha, WANG Xiaojie. Preparation of Chaenomeles speciosa Seed Oil Microcapsule by Spray Drying Technology and Its Properties[J]. Chemistry and Industry of Forest Products, 2018, 38(1): 33-38.

参考文献

[1] 邵文豪,董汝湘,姜景民,等. 皱皮木瓜综合多性状优树选择[J]. 东北林业大学学报,2015(11):46-51. SHAO W H,DONG R X,JIANG J M,et al. Plus tree selection based on comprehensive traits of Chaenomeles speciosa[J]. Journal of Northeast Forestry University,2015(11):46-51.
[2] 刘捷,王文,卢奎,等. 皱皮木瓜多糖的提取及其抗氧化活性研究[J]. 河南工业大学学报:自然科学版,2011,32(1):48-52. LIU J,WANG W,LU K,et al. Extraction and antioxidation activity of polysaccharides from Chaenomeles speciosa (Sweet) Nakai[J]. Journal of Henan University of Technology (Natural Science Edition),2011,32(1):48-52.
[3] ZHANG S Y,HAN L Y,ZHANG H,et al. Chaenomeles speciosa:A review of chemistry and pharmacology[J]. Biomedical Reports,2014,2(1):12-18.
[4] 魏旖琪,姚雷. 皱皮木瓜中总黄酮分离纯化工艺[J]. 上海交通大学学报农业科学版,2014,32(6):71-77. WEI Y Q,YAO L. Optimized extraction and purification of total flavonoids from Chaenomeles speciosa (Sweet) Nakai[J]. Journal of Shanghai Jiaotong University(Agricultural Science),2014,32(6):71-77.
[5] 杨国燕. DSC和Rancimat法测定亚麻籽油氧化稳定性研究[J]. 粮食与油脂,2014(8):29-32. YANG G Y. Study on oxidation stability of flax seed oil by DSC and Rancimat method[J]. Cereals & Oils,2014(8):29-32.
[6] 赵芳,李桂华,罗世龙. 葡萄籽油和亚麻籽油储藏期间氧化对功能性成分影响[J]. 粮食与油脂,2011(5):19-22. ZHAO F,LI G H,LUO S L. Effects of oxygenation on functional ingredients of grape seed oil and linseed oil in the course of preservation[J]. Journal of Cereals & Oils,2011(5):19-22.
[7] 能静,项延楠,孙培龙. 拉曼光谱法检测灵芝孢子油氧化酸败[J]. 食品科学,2015,36(24):200-204. NENG J,XIANG Y N,SUN P L. Rapid detection of oxidative rancidity of ganoderma lucidum spore oil by Raman spectroscopy[J]. Food Science,2015,36(24):200-204.
[8] 刘安然,李宗军. 不同壁材制备油茶籽油微胶囊的研究[J]. 中国粮油学报,2016,31(3):69-73. LIU A R,LI Z J. Research on different wall materials preparation camellia seed oil microcapsules[J]. Journal of the Chinese Cereals and Oils Association,2016,31(3):69-73.
[9] 李懿. 响应面法优化亚麻籽油微胶囊制备工艺[J]. 食品研究与开发,2016,37(6):113-116. LI Y. The response surface method to optimize flax seed oil microcapsule preparation process[J]. Food Research and Development,2016,37(6):113-116.
[10] 刘颖,范婷婷,李笑梅,等. 葡萄籽油提取与微胶囊化研究[J]. 中国粮油学报,2009,24(1):65-69. LIU Y,FAN T T,LI X M,et al. Extraction and microencapsulation of grape seed oil[J]. Journal of the Chinese Cereals and Oils Association,2009,24(1):65-69.
[11] HU L D,ZHANG J L,HU Q F,et al. Microencapsulation of brucea javanica oil:Characterization,stability and optimization of spray drying conditions[J]. Journal of Drug Delivery Science and Tecnology,2016,36:46-54.
[12] 孙兰萍,马龙,张斌,等. 杏仁油微胶囊制备工艺的优化[J]. 农业工程学报,2008,24(9):253-257. SUN L P,MA L,ZHANG B,et al. Optimization of technology for almond oil microencapsulation[J]. Transactions of the Chinese Society of Agricultural Engineering,2008,24(9):253-257.
[13] THIMMA R T,TAMMISHETTI S. Study of complex coacervation of gelatin with sodium carboxymethyl guar gum:Microencapsulation of clove oil and sulphamethoxazole[J]. Journal of microencapsulation,2003,20(2):203-210.
[14] XIAO J X,YU H Y,YANG J. Microencapsulation of sweet orange oil by complex coacervation with soybean protein isolate/gum Arabic[J]. Food chemistry,2011,125(4):1267-1272.
[15] GÓRNAS' P,SIGER A,SEGLIN,A D. Physicochemical characteristics of the cold-pressed Japanese quince seed oil:New promising unconventional bio-oil from by-products for the pharmaceutical and cosmetic industry[J]. Industrial Crops & Products,2013,48(3):178-182.
[16] 赵巍,王军,段长青,等. 喷雾干燥法制备微胶囊化山葡萄籽油粉末油脂[J]. 中国粮油学报,2009,24(12):77-83. ZHAO W,WANG J,DUAN C Q,et al. Manufacturing microcapsules of amur grape seed oil by spray-drying[J]. Journal of the Chinese Cereals and Oils Association,2009,24(12):77-83.
[17] AYSU T,ZEYNEP As,NEVZAT A. Microencapsulation of grape polyphenols using maltodextrin and gum arabic as two alternative coating materials:Development and characterization[J]. Journal of Biotechnolegy,2016,239(10):23-33.
[18] NG S K,CHOONG Y H,TAN C P,et al. Effect of total solids content in feed emulsion on the physical properties and oxidative stability of microencapsulated kenaf seed oil[J]. LWT-food Science and Technology,2014,58(2):627-632.
[19] 李素云,李星科,张华,等. 喷雾干燥法制备芥末油微胶囊化的研究[J]. 中国调味品,2013,38(1):66-68. LI S Y,LI X K,ZHANG H,et al. Study on microencapsulation of mustard oil by spray drying[J]. China Condiment,2013,38(1):66-68.
[20] 李昌宝,吴雪辉,李丽,等. 罗汉果籽油微胶囊化研究[J]. 中国粮油学报,2012,27(11):54-57. LI C B,WU X H,LI L,et al. Study on preparation of grosvenor momordica seed oil microcapsulation[J]. Journal of the Chinese Cereals and Oils Association,2012,27(11):54-57.
[21] 游凤,黄立新,张彩虹,等. 喷雾干燥制备角鲨烯微胶囊的研究[J]. 林产化学与工业,2015,35(5):58-64. YOU F,HUANG L X,ZHANG C H,et al. Study of squalene microcapsule by spray drying technology[J]. Chemistry and Industry of Forest Products,2015,35(5):58-64.
[22] MAHDAVI S A,JAFARI S M,ASSADPOOR E,et al. Microencapsulation optimization of natural anthocyanins with maltodextrin,gum Arabic and gelatin[J]. International Journal of Biological Macromolecules,2016,85(7):379-385.
[23] 刘成祥,王力,苏建辉,等. 牡丹籽油微胶囊的制备及特性研究[J]. 中国油脂,2016,41(11):12-16. LIU C X,WANG L,SU J H,et al. Preparation and property of peony seed oil microcapsule[J]. China Oils and Fats,2016,41(11):12-16.
[24] TIMILSENA Y P,ADHIKARI R,BARROW C J,et al. Microencapsulation of chia seed oil using chia seed protein isolate-chia seed gum complex coacervates[J]. International Journal of Biological Macromolecules,2016,91:347-357.

喷雾干燥法制备皱皮木瓜籽油微胶囊及其性能研究

Preparation of Chaenomeles speciosa Seed Oil Microcapsule by Spray Drying Technology and Its Properties

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