金雀花提取物正丁醇沉淀部分化学成分研究

doi:10.3969/j.issn.0253-2417.2015.03.021

Abstract

Abstract: The chemical constituents of n-butanol-insoluble portion of Parochetus communis Buch extract were studied by acetylation.The aerial part of P.communis was extracted by 75% ethanol and the ethanol extract was suspended in distilled water and successively extracted by petroleum ether,ethyl acetate,and n-butanol.The insoluble portion of n-butanol extract was partly acetylated,then various column chromatographic methods were used for the isolation and purification.The chemical structures of compounds were elucidated on the basis of physicochemical properties and spectral date.Six compounds were isolated from n-butanol-insoluble portion of P.communis Buch and identified as β-sitosterol,1-triacontanol,medicarpin and pratol.All compounds were isolated from the medical plant for the first time.In addition,the solubility of n-butanol-insoluble portion was increased and the polarity of the chemical composition was decreased by acetylation.This method provides a new reference for the separation of high-polar compounds in other plant.

Key words: Parochetus communis Buch., acetylation, n-butanol-insoluble portion, chemical constituents

CLC Number:

TQ35

ZHANG Ni, MU Shu-zhen, WANG Jia-sheng, KONG Qi, YU Zheng-wen. Chemical Constituents of n-Butanol-insoluble Portion from Parochetus communis Buch.Extract[J]. Chemistry and Industry of Forest Products, 2015, 35(3): 121-124.

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Chemical Constituents of n-Butanol-insoluble Portion from Parochetus communis Buch.Extract

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