Chemistry and Industry of Forest Products ›› 2019, Vol. 39 ›› Issue (2): 59-66.doi: 10.3969/j.issn.0253-2417.2019.02.009
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Liming ZHANG1,Rongxue LI1,Xihong HE1,Limin HAO1,2,*(),Zhina HE1,Yujie DAI1
Received:
2018-11-14
Online:
2019-04-25
Published:
2019-05-08
Contact:
Limin HAO
E-mail:hlm2005@163.com
Supported by:
CLC Number:
Liming ZHANG,Rongxue LI,Xihong HE,Limin HAO,Zhina HE,Yujie DAI. Extraction, Purification and Property Analysis of Polysaccharides from Quercus acutissima[J]. Chemistry and Industry of Forest Products, 2019, 39(2): 59-66.
Table 1
Experiment design and results of response surface method analysis"
编号 No. | X1 提取时间/h extraction time | X2 提取温度/℃ extraction temperature | X3 液料比值(mL:g) liquidto solid ratio | Y 得率/% yield |
1 | 3 | 90 | 25 | 1.98 |
2 | 3 | 100 | 20 | 1.56 |
3 | 3 | 90 | 25 | 1.79 |
4 | 3 | 90 | 25 | 1.83 |
5 | 3 | 100 | 30 | 1.65 |
6 | 2 | 80 | 25 | 0.69 |
7 | 3 | 80 | 30 | 1.46 |
8 | 4 | 100 | 25 | 1.53 |
9 | 3 | 90 | 25 | 1.96 |
10 | 2 | 90 | 30 | 0.82 |
11 | 3 | 90 | 25 | 1.86 |
12 | 2 | 90 | 20 | 0.62 |
13 | 3 | 80 | 20 | 1.46 |
14 | 2 | 100 | 25 | 0.78 |
15 | 4 | 90 | 20 | 1.51 |
16 | 4 | 80 | 25 | 1.52 |
17 | 4 | 90 | 30 | 1.69 |
Table 2
Variance analysis of regression equation"
方差来源 source | 平方和 sum of squares | 自由度 df | 均方 mean square | F值 F value | P值 P value | 显著性1) significance |
模型< model | 3.17 | 9 | 0.35 | 51.97 | < 0.0001 | *** |
X1 | 1.45 | 1 | 1.45 | 213.19 | < 0.0001 | *** |
X2 | 0.014 | 1 | 0.014 | 2.01 | 0.0433 | * |
X3 | 0.028 | 1 | 0.028 | 4.07 | 0.0035 | ** |
X1X2 | 4.900×10-3 | 1 | 4.900×10-3 | 0.72 | 0.4233 | |
X1X3 | 1.000×10-3 | 1 | 1.000×10-4 | 0.015 | 0.9067 | |
X2X3 | 2.025×10-3 | 1 | 2.025×10-3 | 0.30 | 0.6016 | |
X12 | 1.30 | 1 | 1.30 | 191.87 | < 0.0001 | *** |
X22 | 0.14 | 1 | 0.14 | 20.86 | 0.0026 | ** |
X32 | 0.12 | 1 | 0.12 | 17.59 | 0.0041 | ** |
残差 residual | 0.047 | 7 | 6.778×10-3 | |||
失拟项 lack of fit | 0.020 | 3 | 6.708×10-3 | 0.98 | 0.4851 | |
纯误差 pure error | 0.027 | 4 | 6.830×10-3 | |||
总和 sum | 3.22 | 16 |
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