Chemistry and Industry of Forest Products ›› 2020, Vol. 40 ›› Issue (3): 69-75.doi: 10.3969/j.issn.0253-2417.2020.03.009
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Chen YANG1,2,Guihua ZHU1,2,Yaming WANG2,Zhihua LIU1,2,Lihong JIANG2,Pei HE1,*()
Received:
2020-01-14
Online:
2020-06-28
Published:
2020-06-29
Contact:
Pei HE
E-mail:hepeisuccess@163.com
CLC Number:
Chen YANG,Guihua ZHU,Yaming WANG,Zhihua LIU,Lihong JIANG,Pei HE. Synthesis of Aluminum Phosphate with Dehydroabietylamine as Structure Directing Agent[J]. Chemistry and Industry of Forest Products, 2020, 40(3): 69-75.
Table 1
Surface area and porosity of the aluminum phosphate synthesized under different condition"
样品 samples | 时间/h duration | 温度/℃ temperature | 比表面积/(m2·g-1) SBET | 平均孔径/nm average pore size | 孔容/(cm3·g-1) pore volume |
a | 4 | 160 | 19.18 | 5.24 | 0.05 |
c | 4 | 180 | 260.80 | 3.23 | 0.58 |
d | 4 | 190 | 158.38 | 3.03 | 0.37 |
e | 4 | 200 | 113.33 | 3.88 | 0.26 |
f | 4 | 210 | 73.84 | 3.92 | 0.17 |
g | 1 | 170 | 35.77 | 6.13 | 0.07 |
h | 2 | 170 | 79.21 | 5.44 | 0.10 |
i | 3 | 170 | 253.69 | 3.12 | 0.64 |
j(b) | 4 | 170 | 272.00 | 3.01 | 0.69 |
k | 5 | 170 | 275.41 | 3.02 | 0.69 |
Table 2
Structural properties of the aluminum phosphates synthesized with different raw materials"
结构导向剂 SDA | 溶剂 solvent | 晶型 phase | 形貌 morphology | 比表面积/ (m2·g-1) SBET | 孔容/ (cm3·g-1) pore volume | 平均孔径/nm pore size | 文献 reference |
去氢枞胺 dehydroabietyla mine | 蒎烯 pinene | 无定形/鳞石英 amorphous/tridymite | 绵状聚集 sticky morphology | 272 | 0.7 | 3.01 | 本研究 present |
杂环芳胺 heterocyclic aromatic a mine | 离子液体 [BMIm]Br | 无定形/CHA amorphous/CHA | 棒状聚集 stick-like shape | [ | |||
芳香分子 aromatic molecule | 水 H2O | 无定形/LTA amorphous/LTA | 菱形 rhombohedral | 600 | [ | ||
三乙胺 triethyla mine | 蒎烯 pinene | AFI型 AFI topology | 棱柱状 prism shape | 297 | 0.3 | 3.3 | [ |
三乙醇胺 triethanola mine | 蒎烯 pinene | 鳞石英 tridymite | 片状 flaky morphology | 129 | 0.1 | 2.5 | [ |
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