Chemistry and Industry of Forest Products ›› 2021, Vol. 41 ›› Issue (3): 85-94.doi: 10.3969/j.issn.0253-2417.2021.03.012
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Jie GUO, Huan WANG, Qi ZHANG, Ke SONG()
Received:
2020-09-30
Online:
2021-06-28
Published:
2021-07-01
Contact:
Ke SONG
E-mail:kesong0608@163.com
CLC Number:
Jie GUO, Huan WANG, Qi ZHANG, Ke SONG. Separation and Identification of Flavonoids from Leaves of Nageia nagi(Thunberg) Kuntze[J]. Chemistry and Industry of Forest Products, 2021, 41(3): 85-94.
Table 1
Adsorption and desorption properties of four types of resins"
树脂 resins | 粒径/mm granularity | 总黄酮total flavonoids | 穗花杉双黄酮amentoflavone | |||
Ea/% | Ed/% | Ea/% | Ed/% | |||
PLA-1 | 0.550~1.180 | 86.38 | 31.82 | 79.44 | 29.64 | |
PLA-2 | 0.250~0.550 | 88.14 | 35.77 | 81.08 | 30.74 | |
D101 | 0.300~1.200 | 80.22 | 64.07 | 62.68 | 56.80 | |
AB-8 | 0.315~1.205 | 82.39 | 73.31 | 69.25 | 60.14 |
Table 2
Comparison on the loading solution with different concentrations"
质量浓度/(g·L-1) mass concentration | 总黄酮的吸附率/% adsorption rates of total flavonoids | 穗花杉双黄酮的吸附率/% adsorption rate of amentoflavone | |||
PLA-2 | AB-2 | PLA-2 | AB-2 | ||
0.5 | 93.14 | 88.61 | 93.55 | 93.55 | |
1.0 | 94.75 | 89.22 | 96.33 | 96.33 | |
1.5 | 94.88 | 90.13 | 96.68 | 96.68 | |
3.0 | 90.16 | 87.60 | 98.57 | 94.68 | |
4.0 | 86.77 | 83.87 | 83.47 | 80.41 |
Table 3
Comparison on the eluents with different concentrations"
乙醇体积分数/% ethanel volume fraction | 总黄酮的解吸率/% desorption rates of total flavonoids | 穗花杉双黄酮的解吸率/% desorption rates of amentoflavone | |||
PLA-2 | AB-8 | PLA-2 | AB-8 | ||
50 | 20.53 | 61.92 | 4.98 | 10.36 | |
60 | 28.25 | 72.32 | 16.74 | 32.46 | |
70 | 34.53 | 84.79 | 38.12 | 71.21 | |
80 | 45.53 | 91.19 | 62.66 | 95.37 | |
90 | 44.27 | 91.87 | 66.18 | 96.43 |
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