›› 2008, Vol. 28 ›› Issue (5): 21-25.
• 研究报告 • Previous Articles Next Articles
LI Xing-di, CHEN Yu-xiang, ZHAO Zhen-dong, BI Liang-wu, GU Yan, LI dong-mei, WANG Jing
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Abstract: Taking advantage of the selectively crystalline specialty of 2-amino-2-methyl-1-propanol toward isopimaric acid, butanolidine isopimarate (2-amino-2-methyl-1-propanol isopimaric acid salt) was prepared by reacting 2-amino-2-methyl-1-propanol with thermally isomerized slash pine rosin that was freshly prepared from oleoresin or rosin, then purified by multi-recrystallization. Thereafter, isopimaric acid was isolated from the butanolidine isopimarate by acidic decomposition in a yield of 10.1% based on the rosin, with purity of 95.4% isopimaric acid. The isolation yield of isopimaric acid is 42.2% based on its content in rosin.
Key words: slash pine oleoresin, slash pine rosin, isopimaric acid, butanolidine isopimarate, multi-recrystallization
CLC Number:
TQ351.471
LI Xing-di;CHEN Yu-xiang;ZHAO Zhen-dong;BI Liang-wu;GU Yan;LI dong-mei;WANG Jing. New Process for Isolation and Preparation of Isopimaric Acid[J]. , 2008, 28(5): 21-25.
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