Chemistry and Industry of Forest Products ›› 2019, Vol. 39 ›› Issue (6): 102-108.doi: 10.3969/j.issn.0253-2417.2019.06.014
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Zhexuan LÜ,Weiwei ZHANG,Dandan LIU,Liwei ZHU,Jianxin JIANG*()
Received:
2019-06-05
Online:
2019-12-28
Published:
2019-12-21
Contact:
Jianxin JIANG
E-mail:jiangjx@bjfu.edu.cn
Supported by:
CLC Number:
Zhexuan LÜ,Weiwei ZHANG,Dandan LIU,Liwei ZHU,Jianxin JIANG. Extraction Technology and Surface Tension Characterization of Gymnocladus chinensis Saponin[J]. Chemistry and Industry of Forest Products, 2019, 39(6): 102-108.
Table 1
Design and results of Box-Behnken experimental"
序号 No. | X1 提取温度/℃ extraction temperature | X2 提取时间/h extraction time | X3 液料比值(mL:g) liquid-solid ratio | Y 得率/% yield |
1 | 60 | 12 | 12 | 25.67 |
2 | 65 | 14 | 12 | 25.06 |
3 | 70 | 12 | 8 | 25.15 |
4 | 65 | 12 | 10 | 26.98 |
5 | 65 | 12 | 10 | 27.06 |
6 | 65 | 10 | 12 | 24.98 |
7 | 65 | 12 | 10 | 26.69 |
8 | 65 | 12 | 10 | 26.74 |
9 | 70 | 12 | 12 | 25.47 |
10 | 65 | 10 | 8 | 25.72 |
11 | 70 | 10 | 10 | 25.86 |
12 | 60 | 14 | 10 | 26.12 |
13 | 60 | 10 | 10 | 24.95 |
14 | 60 | 12 | 8 | 25.17 |
15 | 65 | 14 | 8 | 24.97 |
16 | 70 | 14 | 10 | 24.68 |
Table 2
The table of variance analysis"
方差来源 sources of variance | 平方和 sum of squares | 自由度 df | 均方 mean square | F值 F value | P值 P value | 显著性1) significance |
模型model | 9.02 | 9 | 1.00 | 13.85 | 0.0023 | ** |
X1 | 0.070 | 1 | 0.070 | 0.97 | 0.3623 | |
X2 | 0.058 | 1 | 0.058 | 0.80 | 0.4058 | |
X3 | 3.613×10-3 | 1 | 3.613×10-3 | 0.050 | 0.8306 | |
X1X2 | 1.38 | 1 | 1.38 | 19.08 | 0.0047 | ** |
X1X3 | 8.100×10-3 | 1 | 8.100×10-3 | 0.11 | 0.7493 | |
X2X3 | 0.17 | 1 | 0.17 | 2.38 | 0.1738 | |
X12 | 1.64 | 1 | 1.64 | 22.74 | 0.0031 | ** |
X22 | 2.71 | 1 | 2.71 | 37.52 | 0.0009 | *** |
X32 | 2.97 | 1 | 2.97 | 41.01 | 0.0007 | *** |
残差residual | 0.43 | 6 | 0.072 | 3.45 | 0.1680 | |
失拟项lack of fit | 0.34 | 3 | 0.11 | |||
纯误差pure error | 0.097 | 3 | 0.032 | |||
总和sum | 9.45 | 15 |
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