5-去氢枞基-1,3,4-噻二唑衍生物的合成和除草活性

›› 2011, Vol. 31 ›› Issue (1): 1-8.

• 研究报告 • Next Articles

Synthesis and Herbicidal Activity of 5-Dehydroabietyl- 1,3,4-thiadiazole Derivatives

DUAN Wen-gui¹, DUAN Wen-gui¹, LI Xing-ren^1,2, MA Xian-li¹, MO Qi-jin¹, XU Xue-tang¹

1. College of Chemistry and Chemical Engineering, Guangxi University, Nanning 530004, China;2. College of Pharmacy, Guilin Medical University, Guilin 541004, China

Received:2010-07-29 Revised:1900-01-01 Online:2011-02-28 Published:2011-02-28

Abstract

Abstract: In order to search for novel compounds with higher biological activity, a series of new dehydro-abietic acid derivatives bearing 1,3,4-thiadiazole moieties were designed and synthesized. Eight title compounds of 5-dehydroabietyl-2-substituted amino-1,3,4-thiadiazoles 5(a-h) were synthesized by the cyclization of 1-dehydroabietacyl-4-substituted thiosemicarbazides 4(a-h) under the catalysis of phosphoric acid. All the title compounds were analyzed and characterized by means of IR, UV, EI-MS,¹HNMR,¹³CNMR, and elemental analysis. The preliminary bioassay showed that all these title compounds exhibited excellent growth inhibition against rape(Brassica campestris) and a certain inhibition against barnyard grass Echinochloa crusgalli(L.).

Key words: dehydroabietic acid, 4-thiadiazole, synthesis, herbicidal activity

CLC Number:

TQ351

DUAN Wen-gui;DUAN Wen-gui;LI Xing-ren;MA Xian-li;MO Qi-jin;XU Xue-tang. Synthesis and Herbicidal Activity of 5-Dehydroabietyl- 1,3,4-thiadiazole Derivatives[J]. , 2011, 31(1): 1-8.

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Synthesis and Herbicidal Activity of 5-Dehydroabietyl- 1,3,4-thiadiazole Derivatives

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