Welcome to Chemistry and Industry of Forest Products,

›› 2007, Vol. 27 ›› Issue (04): 42-46.

• 研究报告 • Previous Articles     Next Articles

A New Method of Purifying Abietic Acid

HAN Chun-rui, SONG Zhan-qian, SHANG Shi-bin   

  1. Institute of Chemical Industry of Forest Products, CAF;Key and Open Lab. on Forest Chemical Engineering, SFA, Nanjing 210042, China
  • Received:2006-08-14 Revised:1900-01-01 Online:2007-08-30 Published:2007-08-30

Abstract: Abietic acid of 90.91% purity was obtained by amine salt method, using self-prepared amine A as raw material and 95% ethyl alcohol as recrystallization solvent. The method is economic and environmentally friendly because of the low price of amine A and small consumption of recrystallization solvent. Sample was characterized by 1H NMR, UV, IR and GC-MS methods.Purifications of abietic acid with isopropylamine, cyclohexylamine, octadecyl primaryamine, di-n-butylamine, triethylamine, and amine A were studied. The effects of carbon numbers of amines and primary, secondary, tertiary amines on purifying process were analyzed. The abietic acid with purity of 90% could be stored for 2 months at 5 kPa and -15℃.

Key words: abietic aid, rosin acid, purify, amine

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