毛竹竹青和竹黄细胞壁中阿魏酸和对香豆酸定量分析

doi:10.3969/j.issn.0253-2417.2016.03.003

Abstract

Abstract: Moderate alkali hydrolysis and acid hydrolysis were applied to quantitatively determine the amount of ferulic and p-coumaric acid in the cell wall of Moso bamboo green and bamboo yellow. The results indicated that 3.07% of ferulic acid and 5.91% of p-coumaric acid were found in the bamboo green cell wall. And 1.61% ferulic acid and 4.64% p-coumaric acid were ester-linked to the bamboo green cell wall components, while 1.46% ferulic acid and 1.27% p-coumaric acid were ether-linked to the cell wall component. For bamboo yellow, there were 3.11% of ferulic acid and 5.51% of p-coumaric acid. The amounts of ester-linked and ether-linked ferulic acid were 1.71% and 1.40%, respectively. And the amounts of ester-linked and ether-linked p-coumaric acid were 4.34% and 1.17%, respectively. Two-dimensional heteronuclear single quantum correlation nuclear magnetic resonance(2D-HSQC NMR) confirmed that the ester-linked ferulic and p-coumaric acid in the alkaline-soluble lignins of bamboo green and bamboo yellow might be esterified in the γ position of β-O-4 aryl ether bonds in the lignin.

Key words: bamboo green, bamboo yellow, ferulic acid, p-coumaric acid, quantitative determination, 2D-HSQC NMR

CLC Number:

TQ35

HUANG Cao-xing, HE Juan, MIN Dou-yong, LI Xin, DU Li-ting, YONG Qiang. Quantitative Determination of Ferulic and p-Coumaric Acids in Cell Wall of Moso Bamboo Green and Bamboo Yellow[J]. Chemistry and Industry of Forest Products, 2016, 36(3): 16-22.

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Quantitative Determination of Ferulic and p-Coumaric Acids in Cell Wall of Moso Bamboo Green and Bamboo Yellow

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[1]	HUANG Cao-xing, HE Juan, MIN Dou-yong, LI Xin, YONG Qiang. Isolation and Characterization of Hemicellulose from Moso Bamboo Green and Bamboo Yellow [J]. Chemistry and Industry of Forest Products, 2015, 35(5): 29-36.
[2]	WU Dong-mei;CHEN Jia-hong;WANG Yong-mei;WU Zai-song . Study on Quantitative Determination of 1,2,3-Trimethoxybenzene [J]. , 2007, 27(6): 95-98.