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›› 2008, Vol. 28 ›› Issue (04): 112-114.

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Determination of Trace Iron in 2,3,4,4′-Tetrahydroxybenzophenone by Graphite Furnace Atomic Absorption Spectrometry

WANG Wei-ru1, HUANG Jia-ling1,2, WANG Jian-sheng1, JING Xia1, CHEN Wen-wen1,2   

  1. 1. Nanjing Longyuan Natural Polyphenol Synthesis Factory, Nanjing 210032, China;2. Institute of Chemical Industry of Forest Products, CAF;Key and Open Lab.on Forest Chemical Engineering, SFA, Nanjing 210042, China
  • Received:2008-03-27 Revised:1900-01-01 Online:2008-08-30 Published:2008-08-30

Abstract: A determination method of trace iron in 2,3,4,4'-tetrahydroxybenzophenone by graphite furnace atomic absorption spectrometry is established. The optimum condition of graphite temperature and electric current of hollow cathode lamp were investigated. Determination conditions were: drying temperature 120℃, ashing temperature 700℃, atomization temperature 2400℃,electric current of hollow cathode lamp 3mA. There was a good linearity in range of 2.5-10.0μg/L. Relative standard deviation(RSD) was 1.99%, and recovery rate was 94.2%. This method was accurate and reproducible, and suitable for determination of trace iron in 2,3,4,4'-tetrahydroxybenzophenone.

Key words: atomic absorption spectrometry, graphite furnace, 4'-tetrahydroxybenzophenone, trace iron

CLC Number: