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林产化学与工业

林产化学与工业 ›› 2012, Vol. 32 ›› Issue (5): 115-119.

• 1研究报告 • 上一篇    下一篇

顶空固相微萃取-气相色谱/质谱法分析不同材质木片中的挥发性成分

王慧1, 曾熠程1, 侯英2, 翁瑞杰1, 杨晶津1, 朱勇1, 周文忠2, 杨燕2   

  1. 1. 红云红河烟草(集团)有限责任公司, 云南 昆明 650000;2. 云南瑞升 烟草技术(集团)有限公司, 云南 昆明 650106
  • 收稿日期:2011-11-15 修回日期:1900-01-01 出版日期:2012-10-30 发布日期:2012-10-30

Analysis of Different Volatile Constituents in the Wood Material by Headspace Solid Phase Microextraction-gas Chromatography-mass Spectrometry

WANG Hui1, ZENG Yi-cheng1, HOU Ying2, WENG Rui-jie1, YANG Jing-jin1, ZHU Yong1, ZHOU Wen-zhong2, YANG Yan2   

  1. 1. Hongyun Honghe Tobacco (Group) Co.,Ltd., Kunming 650000, China;2. YunNan Reascend Tobacco Technology(Group)Co., Ltd., Kunming 650106, China
  • Received:2011-11-15 Revised:1900-01-01 Online:2012-10-30 Published:2012-10-30

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摘要： 采用顶空固相微萃取-气相色谱-质谱法分析橡木、西南桦木、枫木、松木、铁杉这5种木片中的挥发性成分。结果显示,5种木片均检出了45种挥发性成分,其中橡木木片鉴定出49种,西南桦木片鉴定出45种,枫木木片鉴定出47种,松木木片鉴定出50种,铁杉木片鉴定出47种。其中橡木木片中的挥发性化合物如5-甲基-2-糠醛、糠醛、香叶基丙酮、 β-紫罗兰酮与卷烟中典型代表香味成分相同,这些香味成分可能有助于使储存在其中的烟丝的香味成分含量增加并对其感官品质起到一定的提升作用。

关键词: 顶空固相微萃取法, 气相色谱-质谱法, 木片, 挥发性成分

Abstract: Headspace solid phase microextraction-gas chromatography/mass spectrometry was used to analyze volatile constituents in the oak chips, southwest birch chips, maple chips, pine chips and hemlock chips. The results showed that forty to fifty kinds of volatile constituents in five kinds of wood were detected. There were forty-nine kinds in oak chips, forty-five kinds in southwest birch chips, forty-seven kinds in maple chips, fifty kinds in pine chips and forty-seven kinds in hemlock chips.These data will provide a theoretical basis and technical support for their applications in production. In oak wood chips, the volatile constituents such as 5-methyl-2-furancarboxaldehyde, furfural, geranyl acetone,and β-ionone were the same as cigarette typical representative flavor components. The flavor components may contribute to the increase of stored tobacco flavor ingredients and enhance its sensory quality.

Key words: headspace solid phase microextraction(HS-SPME), gas chromatography-mass spectrometry(GC-MS), wood chip, volatile constituents

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