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›› 2012, Vol. 32 ›› Issue (1): 39-42.

• 研究报告 • Previous Articles     Next Articles

Synthesis and Structural Analysis of Hydronopol and Its Halides

ZHAO Ling-hua1, XIAO Zhuan-quan2, CHEN Jin-zhu3, WANG Zong-de1, FAN Guo-rong1, CHEN Shang-xing1   

  1. 1. College of Forestry,Jiangxi Agricultural University, Nanchang 330045, China;2. College of Chemistry, Jiangxi Normal University, Nanchang 330027, China;3. College of Science, Jiangxi Agricultural University, Nanchang 330045, China
  • Received:2011-05-16 Revised:1900-01-01 Online:2012-02-28 Published:2012-02-28

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Abstract: Hydronopol was prepared by the hydrogenation of nopol, which was synthesized from β-pinene and paraformaldehyde in the presence of Raney Ni. Hydronopyl chloride and hydronopyl bromide were synthesized from hydronopol with thionyl chloride, sodium bromide and sulfuric acid, respectively. Hydronopyl iodide was synthesized from hydronopyl chloride and sodium iodide. Identification and structural analysis were done using IR,1HNMR,13CNMR and MS methods .

Key words: nopol, hydronopol, halides, structural analysis

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