Welcome to Chemistry and Industry of Forest Products,

›› 2010, Vol. 30 ›› Issue (3): 73-77.

• 研究报告 • Previous Articles     Next Articles

Study on Technology of Supercritical CO2 Extraction of Perilla Oil and Its Integrated Inclusion with α-Cyclodextrin

SUN Xin-chao1, YANG Bo1, XU Yuan2, YANG Jian1, ZHAO Yu-lin2, WANG Jing1, WANG Cui-min1   

  1. 1. College of Life Science and Technology, Kunming University of Science and Technology, Kunming 650224, China;2. College of Chemical Engineering, Kunming University of Science and Technology, Kunming 650224, China
  • Received:2009-07-16 Revised:1900-01-01 Online:2010-06-30 Published:2010-06-30

Abstract: Perilla oil was extracted with supercritical CO2 extraction, and the supercritical conditions for integrated inclusion of perilla oil was researched using β-cyclodextrin microcapsulation technology. The results show that the optimum conditions were: supercritical extraction pressure of perilla oil 23MPa, the optimum β-cyclodextrin inclusion supercritical pressure 12MPa, inclusion reaction time 180min, inclusion reaction temperature 55℃, extractant CO2 flow rate 40L/min. α-Lindenic acid inclusion rate is 16.37%, the maximum ratio of mass fraction of β-cyclodextrin/perilla oil is 16.42%, the highest molar complexation ratio (β-cyclodextrin/perilla oil) amounts to 1.84:1 (molar ratio of material), average mass fraction of perilla oil/β-cyclodextrin is 13.94%, and the average complexation ratio is 1.55:1(molar ratio of material).

Key words: perilla oil, supercritical extraction, supercritical inclusion, β-cyclodextrin, supercritical microencapsulation technology

CLC Number: