Welcome to Chemistry and Industry of Forest Products,

›› 2012, Vol. 32 ›› Issue (1): 85-88.

• 研究报告 • Previous Articles     Next Articles

Analysis of the Chemical Constituents by Supercritical CO2 Extraction from Dried Flower of Syringa oblata Lindl.

JIAO Shu-qing, ZONG Xi-ming, ZHANG Nan-nan, TAO Yi   

  1. College of Pharmacy,Jiamusi University,Heilongjiang Province the Key Laboratory of Biological Medicine Formulation, Jiamusi 154007, China
  • Received:2011-03-30 Revised:1900-01-01 Online:2012-02-28 Published:2012-02-28

Abstract: Dried flowers of Syringa oblata Lindl. were extracted by supercritical CO2 and the extracts were separated in separators Ⅰ(8 MPa,45 ℃) and Ⅱ(5 MPa,35 ℃). The chemical compositions of the extract from the separators Ⅰ and Ⅱ were analysed by GC-MS. 21 Different compounds in the obtained extract from the separatorⅠwere identified and were mainly long-chain alkane (57.14 %) with nonacosane and 2,6,10,14-tetramethyl hexadecane as major compounds. Forty compounds in the extract from the separator Ⅱ were identified and were mainly oxy-compounds with hexadecanoic acid and 9,12-octadecadienoic acid (Z,Z) as major components, such as alcohols, ketones, aldehydes, acids and esters accounting for 67.5 %. The supercritical CO2 extracts can be separated in certain extent by the two-stage separation. Temperature and pressure are the key factors for the separation results.

Key words: Syringa oblata Lindl. flowers, extract, GC-MS, supercritical CO2 extraction

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