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林产化学与工业 ›› 2004, Vol. 24 ›› Issue (S1): 73-76.

• 研究报告 • 上一篇    下一篇

微波辅助提取兴安落叶松木材中阿拉伯半乳聚糖的工艺研究

方桂珍, 黄占华, 刘宝亮   

  1. 东北林业大学 材料科学与工程学院, 黑龙江 哈尔滨 150040
  • 收稿日期:2003-07-25 修回日期:1900-01-01 出版日期:2004-10-20 发布日期:2004-10-20

MICROWAVE-ASSISTED EXTRACTION OF ARABINOGALACTAN FROM LARIX GMELINII R.WOOD

FANG Gui-zhen, HUANG Zhan-hua, LIU Bao-liang   

  1. College of Material Science and Engineering, Northeast Forestry University, Harbin 150040, China
  • Received:2003-07-25 Revised:1900-01-01 Online:2004-10-20 Published:2004-10-20

摘要: 以兴安落叶松(Larix gmelinii Rupr.)木材的加工剩余物为原料,以水为溶剂,微波辅助提取阿拉伯半乳聚糖。通过对影响提取率的主要因素微波作用时间、微波功率、料液比和木粉粒度等进行正交试验,分析得出微波辅助提取阿拉伯半乳聚糖的较佳工艺参数为10.0g兴安落叶松木粉,微波功率210W,微波作用时间35min,料液质量比1:35,木粉粒度0.2~0.3mm时,阿拉伯半乳聚糖提取率17.47%,比传统水浴浸提法高1.6%,时间仅为原来的1/10。用红外和紫外光谱分析两种方法所得产物的化学结构相同,微波辅助提取的粗糖中杂质含量比传统水浴法低。实验结果表明,对于兴安落叶松木材中阿拉伯半乳聚糖的提取,微波辅助提取优于传统水浴浸提法。

关键词: 微波辅助提取, 兴安落叶松木材, 阿拉伯半乳聚糖, 正交试验

Abstract: Arabinogalactan was extracted from processing residue of Larix gmelinii Rupr. wood as raw material. Water was used as solvent, assisted by microwave irradiation. In the experiments, parameters affecting extraction of arabinogalactan, namely: microwave power, irradiation time, wood flour granularity, the ratio of liquid to material were analysed with orthogonal experiment of microwave-assisted extraction. The optimum parameters were obtained as follows: microwave power 210 W, irradiation time 35 min, ratio of liquid to material 1:35, wood flour granularity 0.2-0.3 mm. The extract yield of arabinogalactan was 17.47%, which was 1.6% higher than traditional water extraction, with time only 1/10 of the latter. The products obtained from both extraction methods were identical in chemical structure by IR analyses. The impurity content of raw arabinogalactan by microwave extraction was lower than that by traditional water extraction. The experiment results showed that microwave-assisted extraction is superior to traditional water extraction for extraction of arabinogalactan from Larix gmelinii R. wood.

Key words: microwave-assisted extraction, Larix gmelinii Rupr.wood, arabinogalactan, orthogonal experiment

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